E-Liquid Test Results for 03 December 2013 (1212-39R) - Enthalpy Labs

E-Liquid Test Results for 03 December 2013 (1212-39R) - Enthalpy Labs

Standards Legend
Component / Element	Protocol MDL*	Tolerance
Nicotine Concentration	GC/FID Analysis 0.1 mg/ml	± 10%
Diethylene glycol (DEG)	GC/FID Analysis 2.23 µg/ml (ppm)	No Detection
Acetaldehyde	HPLC/UV Analysis 0.640 µg/ml (ppm)	< 100 µg/ml (ppm)
Acetoin	HPLC/UV Analysis 0.841 µg/ml (ppm)	None Set (Informational)
Diacetyl (2,3-Butanedione)	HPLC/UV Analysis 0.742 µg/ml (ppm)	Non-Detection Goal < 22 µg/ml no disclosure < 100 µg/ml (ppm) disclosure > 100 µg/ml (ppm) is Fail
Formaldehyde	HPLC/UV Analysis 0.846 µg/ml (ppm)	< 30 µg/mL (ppm)
Acetyl Propionyl (2,3-Pentanedione )	HPLC/UV Analysis 0.840 µg/ml (ppm)	Non-Detection Goal < 45 µg/ml no disclosure < 100 µg/ml (ppm) disclosure > 100 µg/ml (ppm) is Fail
pH Level	Karl Fischer Analysis	Target Levels (Informational) 5.0 to 8.5
% Water	Karl Fischer Analysis	None Set (Informational)

* MDL - Minimum Detection Limit. The MDL will remain relatively constant but can vary slightly from test to test depending on the calibration of the equipment.

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03 December 2013 (1213-39R)

Flavour	Northern 7 Tobacco 2.4%	Cuban Cigar 2.4%	Sweet Honey Cigar 1.8%
Sample ID	ECTA002-007	ECTA002-008	ECTA002-009
Enthalpy Code	1213-39-01	1213-39-02	1213-39-03
Nicotine Concentration MDL: 0.100 mg/ml	25.0 mg/ml	24.1 mg/ml	19.2 mg/ml
Diethylene glycol (DEG) MDL: 11.1 µg/ml	ND	ND	ND
Acetaldehyde MDL: 1.21 µg/ml	1.46 µg/ml	ND	1.51 µg/ml
Crotonaldehyde MDL: 1.15 µg/ml	ND	ND	ND
Diacetyl (2,3-Butanedione) MDL: 1.40 µg/ml	ND	ND	ND
Formaldehyde MDL: 0.846 µg/ml	ND	2.92 µg/ml	3.11 µg/ml
pH	8.55	8.85	8.46
% Water	0.32%	0.64%	0.32%
Flavour	Bluemont Tobacco 1.8%	Cranberry Champagne 1.2%	Butter Rum Tobacco 1.2%
Sample ID	ECTA002-010	ECTA002-011	ECTA002-012
Enthalpy Code	1213-39-04	1213-39-05	1213-39-06
Nicotine Concentration MDL: 0.100 mg/ml	18.6 mg/ml	12.3 mg/ml	12.4 mg/ml
Diethylene glycol (DEG) MDL: 11.1 µg/ml	ND	ND	ND
Acetaldehyde MDL: 1.21 µg/ml	ND	ND	3.98 µg/ml
Crotonaldehyde MDL: 1.15 µg/ml	21.3 µg/ml	ND	ND
Diacetyl (2,3-Butanedione) MDL: 1.40 µg/ml	ND	ND	ND
Formaldehyde MDL: 0.846 µg/ml	2.17 µg/ml	3.01 µg/ml	13.8 µg/ml
pH	7.36	8.20	6.01
% Water	0.40%	0.50%	1.62%
Flavour	Coumarin Pipe 0.8%	Root Beer 0.8%	Rich Caramel Non-Nic
Sample ID	ECTA002-013	ECTA002-014	ECTA002-015
Enthalpy Code	1213-39-07	1213-39-08	1213-39-09
Nicotine Concentration MDL: 0.100 mg/ml	7.9 mg/ml	8.04 mg/ml	ND
Diethylene glycol (DEG) MDL: 11.1 µg/ml	ND	ND	ND
Acetaldehyde MDL: 1.21 µg/ml	ND	ND	2.56 µg/ml
Crotonaldehyde MDL: 1.15 µg/ml	ND	ND	ND
Diacetyl (2,3-Butanedione) MDL: 1.40 µg/ml	ND	ND	ND
Formaldehyde MDL: 0.846 µg/ml	3.39 µg/ml	2.80 µg/ml	19.2 µg/ml
pH	8.35	8.73	5.81
% Water	1.39%	0.28%	1.95%
Flavour	Mr. Pepper Non-Nic
Sample ID	ECTA002-016
Enthalpy Code	1213-39-10
Nicotine Concentration MDL: 0.100 mg/ml	1.88 mg/ml See Actions
Diethylene glycol (DEG) MDL: 11.1 µg/ml	ND
Acetaldehyde MDL: 1.21 µg/ml	ND
Crotonaldehyde MDL: 1.15 µg/ml	ND
Diacetyl (2,3-Butanedione) MDL: 1.40 µg/ml	ND
Formaldehyde MDL: 0.846 µg/ml	4.29 µg/ml
pH	3.85
% Water	2.10%

ND: Non Detect or analytical result below the MDL.
J: Results flagged "J" are below the Lower Curve Limit, above the MDL, and are considered estimates.

ACTIONS TAKEN:

Mr. Pepper Non-Nic, more than ± 10% variation - All liquids of that batch number were immediately pulled from stock. QA process review was performed on Non-Nic production for possible causes of cross-contamination.

The pages of the report showing these results are below:

Cover Page	Report Page 4	Report Page 5

Report Page 6	Report Page 7	Report Page 8

Report Page 9

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