E-Liquid Test Results for 03 December 2013 (1212-39R) - Enthalpy Labs

E-Liquid Test Results for 03 December 2013 (1212-39R) - Enthalpy Labs

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Standards Legend
Component / Element Protocol
MDL*
Tolerance
Nicotine Concentration GC/FID Analysis
0.1 mg/ml
± 10%
Diethylene glycol (DEG) GC/FID Analysis
2.23 µg/ml (ppm)
No Detection
Acetaldehyde HPLC/UV Analysis
0.640 µg/ml (ppm)
< 100 µg/ml (ppm)
Acetoin HPLC/UV Analysis
0.841 µg/ml (ppm)
None Set (Informational)
Diacetyl
(2,3-Butanedione)
HPLC/UV Analysis
0.742 µg/ml (ppm)
Non-Detection Goal
< 22 µg/ml no disclosure
< 100 µg/ml (ppm) disclosure
> 100 µg/ml (ppm) is Fail
Formaldehyde HPLC/UV Analysis
0.846 µg/ml (ppm)
< 30 µg/mL (ppm)
Acetyl Propionyl
(2,3-
Pentanedione)
HPLC/UV Analysis
0.840 µg/ml (ppm)
Non-Detection Goal
< 45 µg/ml no disclosure
< 100 µg/ml (ppm) disclosure
> 100 µg/ml (ppm) is Fail
pH Level Karl Fischer Analysis Target Levels (Informational)
5.0 to 8.5
% Water Karl Fischer Analysis None Set (Informational)

* MDL - Minimum Detection Limit. The MDL will remain relatively constant but can vary slightly from test to test depending on the calibration of the equipment.

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03 December 2013 (1213-39R)

Flavour Northern 7 Tobacco
2.4%
Cuban Cigar
2.4%
Sweet Honey Cigar
1.8%
Sample ID ECTA002-007 ECTA002-008 ECTA002-009
Enthalpy Code 1213-39-01 1213-39-02 1213-39-03
Nicotine Concentration
MDL: 0.100 mg/ml
25.0 mg/ml 24.1 mg/ml 19.2 mg/ml
Diethylene glycol (DEG)
MDL: 11.1 µg/ml
ND ND ND
Acetaldehyde
MDL: 1.21 µg/ml
1.46 µg/ml ND 1.51 µg/ml
Crotonaldehyde
MDL: 1.15 µg/ml
ND ND ND
Diacetyl (2,3-Butanedione)
MDL: 1.40 µg/ml
ND ND ND
Formaldehyde
MDL: 0.846 µg/ml
ND 2.92 µg/ml 3.11 µg/ml
pH 8.55 8.85 8.46
% Water 0.32% 0.64% 0.32%
Flavour Bluemont Tobacco
1.8%
Cranberry Champagne
1.2%
Butter Rum Tobacco
1.2%
Sample ID ECTA002-010 ECTA002-011 ECTA002-012
Enthalpy Code 1213-39-04 1213-39-05 1213-39-06
Nicotine Concentration
MDL: 0.100 mg/ml
18.6 mg/ml 12.3 mg/ml 12.4 mg/ml
Diethylene glycol (DEG)
MDL: 11.1 µg/ml
ND ND ND
Acetaldehyde
MDL: 1.21 µg/ml
ND ND 3.98 µg/ml
Crotonaldehyde
MDL: 1.15 µg/ml
21.3 µg/ml ND ND
Diacetyl (2,3-Butanedione)
MDL: 1.40 µg/ml
ND ND ND
Formaldehyde
MDL: 0.846 µg/ml
2.17 µg/ml 3.01 µg/ml 13.8 µg/ml
pH 7.36 8.20 6.01
% Water 0.40% 0.50% 1.62%
Flavour Coumarin Pipe
0.8%
Root Beer
0.8%
Rich Caramel
Non-Nic
Sample ID ECTA002-013 ECTA002-014 ECTA002-015
Enthalpy Code 1213-39-07 1213-39-08 1213-39-09
Nicotine Concentration
MDL: 0.100 mg/ml
7.9 mg/ml 8.04 mg/ml ND
Diethylene glycol (DEG)
MDL: 11.1 µg/ml
ND ND ND
Acetaldehyde
MDL: 1.21 µg/ml
ND ND 2.56 µg/ml
Crotonaldehyde
MDL: 1.15 µg/ml
ND ND ND
Diacetyl (2,3-Butanedione)
MDL: 1.40 µg/ml
ND ND ND
Formaldehyde
MDL: 0.846 µg/ml
3.39 µg/ml 2.80 µg/ml 19.2 µg/ml
pH 8.35 8.73 5.81
% Water 1.39% 0.28% 1.95%
Flavour Mr. Pepper
Non-Nic
Sample ID ECTA002-016
Enthalpy Code 1213-39-10
Nicotine Concentration
MDL: 0.100 mg/ml
1.88 mg/ml
See Actions
Diethylene glycol (DEG)
MDL: 11.1 µg/ml
ND
Acetaldehyde
MDL: 1.21 µg/ml
ND
Crotonaldehyde
MDL: 1.15 µg/ml
ND
Diacetyl (2,3-Butanedione)
MDL: 1.40 µg/ml
ND
Formaldehyde
MDL: 0.846 µg/ml
4.29 µg/ml
pH 3.85
% Water 2.10%

ND: Non Detect or analytical result below the MDL.
J: Results flagged "J" are below the Lower Curve Limit, above the MDL, and are considered estimates.

ACTIONS TAKEN:

  • Mr. Pepper Non-Nic, more than ± 10% variation - All liquids of that batch number were immediately pulled from stock. QA process review was performed on Non-Nic production for possible causes of cross-contamination.

The pages of the report showing these results are below:

Cover Page Report Page 4 Report Page 5
Report Page 6 Report Page 7 Report Page 8
Report Page 9

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