E-Liquid Test Results for 16 July 2013 (0713-116-01) - Enthalpy Labs
E-Liquid Test Results for 16 July 2013 (0713-116-01) - Enthalpy Labs
| Component / Element | Protocol MDL* |
Tolerance | |
|---|---|---|---|
| Nicotine Concentration | GC/FID Analysis 0.1 mg/ml |
± 10% | |
| Diethylene glycol (DEG) | GC/FID Analysis 2.23 µg/ml (ppm) |
No Detection | |
| Acetaldehyde | HPLC/UV Analysis 0.640 µg/ml (ppm) |
< 100 µg/ml (ppm) | |
| Acetoin | HPLC/UV Analysis 0.841 µg/ml (ppm) |
None Set (Informational) | |
| Diacetyl (2,3-Butanedione) |
HPLC/UV Analysis 0.742 µg/ml (ppm) |
Non-Detection Goal
< 22 µg/ml no disclosure
< 100 µg/ml (ppm) disclosure
> 100 µg/ml (ppm) is Fail
|
|
| Formaldehyde | HPLC/UV Analysis 0.846 µg/ml (ppm) |
< 30 µg/mL (ppm) | |
|
Acetyl Propionyl (2,3-Pentanedione) |
HPLC/UV Analysis 0.840 µg/ml (ppm) |
Non-Detection Goal
< 45 µg/ml no disclosure
< 100 µg/ml (ppm) disclosure
> 100 µg/ml (ppm) is Fail
|
|
| pH Level | Karl Fischer Analysis | Target Levels (Informational) 5.0 to 8.5 |
|
| % Water | Karl Fischer Analysis | None Set (Informational) | |
* MDL - Minimum Detection Limit. The MDL will remain relatively constant but can vary slightly from test to test depending on the calibration of the equipment.
16 July 2013 (0713-116-01)
| Flavour | Nicotine Base 10.0% |
Reserve Cigar Non-Nic |
Butterscotch 0.8% |
|---|---|---|---|
| Sample ID | FC-001 | FC-002 | FC-003 |
| Enthalpy Code | 0713-116-1-01 | 0713-116-1-02 | 0713-116-1-03 |
| Nicotine Concentration MDL: 2.04 mg/ml |
98.2 mg/ml | ND | 8.57 mg/ml |
| Diethylene glycol (DEG) MDL: 2.23 µg/ml |
ND | ND | ND |
| Acetaldehyde MDL: 0.595 µg/ml |
3.57 µg/ml | 1.94 µg/ml | 5.91 µg/ml |
| Crotonaldehyde MDL: 0.564 µg/ml |
ND | ND | ND |
| 2,3-Butanedione MDL: 0.718 µg/ml |
ND | ND | |
| Formaldehyde MDL: 0.549 µg/ml |
19.4 µg/ml | 13.5 µg/ml | 4.52 µg/ml |
| pH | 9.18 | 6.95 | 8.08 |
| % Water | 0.48% | 0.86% | 0.55% |
| Flavour | Export Tobacco 1.2% |
Mac Maurier 1.8% |
Mild Tobacco 2.4% |
| Sample ID | FC-004 | FC-005 | FC-006 |
| Enthalpy Code | 0713-116-1-04 | 0713-116-1-05 | 0713-116-1-06 |
| Nicotine Concentration MDL: 2.04 mg/ml |
11.3 mg/ml | 17.8 mg/ml | 24.3 mg/ml |
| Diethylene glycol (DEG) MDL: 2.23 µg/ml |
ND | ND | ND |
| Acetaldehyde MDL: 0.595 µg/ml |
1.75 µg/ml | 2.03 µg/ml | 1.28 µg/ml |
| Crotonaldehyde MDL: 0.564 µg/ml |
6.24 µg/ml | ND | ND |
| 2,3-Butanedione MDL: 0.718 µg/ml |
ND | 2.60 µg/ml | ND |
| Formaldehyde MDL: 0.549 µg/ml |
1.73 µg/ml | 1.64 µg/ml | 1.95 µg/ml |
| pH | 8.57 | 8.58 | 8.42 |
| % Water | 0.86% | 3.84% | 0.66% |
ND: Non Detect or analytical result below the MDL.
J: Results flagged "J" are below the Lower Curve Limit, above the MDL, and are considered estimates.
-
Butterscotch 0.8%, Diacetyl Detection more than 100 ppm - An immediate stop sale and stop production of Butterscotch was initiated. The flavouring that was used was sold by Flavor West. The Butterscotch Flavouring on their webpage had a statement that all of their flavours were Diacetyl (2,3-Butanedione) Free. Obviously, it is not. Upon contacting them about the issue, they removed the statement on their website, for that product. This flavour has been discontinued.The pages of the report showing these results are below:
Cover Page Report Page 4 Report Page 5 
Report Page 6 Report Page 7 Report Page 12 
