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E-Liquid Test Results for 16 July 2013 (0713-116-01) - Enthalpy Labs

E-Liquid Test Results for 16 July 2013 (0713-116-01) - Enthalpy Labs

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Standards Legend
Component / Element Protocol
MDL*
Tolerance
Nicotine Concentration GC/FID Analysis
0.1 mg/ml
± 10%
Diethylene glycol (DEG) GC/FID Analysis
2.23 µg/ml (ppm)
No Detection
Acetaldehyde HPLC/UV Analysis
0.640 µg/ml (ppm)
< 100 µg/ml (ppm)
Acetoin HPLC/UV Analysis
0.841 µg/ml (ppm)
None Set (Informational)
Diacetyl
(2,3-Butanedione)
HPLC/UV Analysis
0.742 µg/ml (ppm)
Non-Detection Goal
< 22 µg/ml no disclosure
< 100 µg/ml (ppm) disclosure
> 100 µg/ml (ppm) is Fail
Formaldehyde HPLC/UV Analysis
0.846 µg/ml (ppm)
< 30 µg/mL (ppm)
Acetyl Propionyl
(2,3-
Pentanedione)
HPLC/UV Analysis
0.840 µg/ml (ppm)
Non-Detection Goal
< 45 µg/ml no disclosure
< 100 µg/ml (ppm) disclosure
> 100 µg/ml (ppm) is Fail
pH Level Karl Fischer Analysis Target Levels (Informational)
5.0 to 8.5
% Water Karl Fischer Analysis None Set (Informational)

* MDL - Minimum Detection Limit. The MDL will remain relatively constant but can vary slightly from test to test depending on the calibration of the equipment.

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16 July 2013 (0713-116-01)

Flavour Nicotine Base
10.0%
Reserve Cigar
Non-Nic
Butterscotch
0.8%
Sample ID FC-001 FC-002 FC-003
Enthalpy Code 0713-116-1-01 0713-116-1-02 0713-116-1-03
Nicotine Concentration
MDL: 2.04 mg/ml
98.2 mg/ml ND 8.57 mg/ml
Diethylene glycol (DEG)
MDL: 2.23 µg/ml
ND ND ND
Acetaldehyde
MDL: 0.595 µg/ml
3.57 µg/ml 1.94 µg/ml 5.91 µg/ml
Crotonaldehyde
MDL: 0.564 µg/ml
ND ND ND
2,3-Butanedione
MDL: 0.718 µg/ml
ND ND 1,797 µg/ml
See Actions
Formaldehyde
MDL: 0.549 µg/ml
19.4 µg/ml 13.5 µg/ml 4.52 µg/ml
pH 9.18 6.95 8.08
% Water 0.48% 0.86% 0.55%
Flavour Export Tobacco
1.2%
Mac Maurier
1.8%
Mild Tobacco
2.4%
Sample ID FC-004 FC-005 FC-006
Enthalpy Code 0713-116-1-04 0713-116-1-05 0713-116-1-06
Nicotine Concentration
MDL: 2.04 mg/ml
11.3 mg/ml 17.8 mg/ml 24.3 mg/ml
Diethylene glycol (DEG)
MDL: 2.23 µg/ml
ND ND ND
Acetaldehyde
MDL: 0.595 µg/ml
1.75 µg/ml 2.03 µg/ml 1.28 µg/ml
Crotonaldehyde
MDL: 0.564 µg/ml
6.24 µg/ml ND ND
2,3-Butanedione
MDL: 0.718 µg/ml
ND 2.60 µg/ml ND
Formaldehyde
MDL: 0.549 µg/ml
1.73 µg/ml 1.64 µg/ml 1.95 µg/ml
pH 8.57 8.58 8.42
% Water 0.86% 3.84% 0.66%

ND: Non Detect or analytical result below the MDL.
J: Results flagged "J" are below the Lower Curve Limit, above the MDL, and are considered estimates.

ACTIONS TAKEN:

  • Butterscotch 0.8%, Diacetyl Detection more than 100 ppm - An immediate stop sale and stop production of Butterscotch was initiated. The flavouring that was used was sold by Flavor West. The Butterscotch Flavouring on their webpage had a statement that all of their flavours were Diacetyl (2,3-Butanedione) Free. Obviously, it is not. Upon contacting them about the issue, they removed the statement on their website, for that product. This flavour has been discontinued.

     

    The pages of the report showing these results are below:

    Cover Page Report Page 4 Report Page 5
    Report Page 6 Report Page 7 Report Page 12

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