E-Liquid Test Results for 16 May 2014 (0514-129) - Enthalpy Labs

E-Liquid Test Results for 16 May 2014 (0514-129) - Enthalpy Labs

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Standards Legend
Component / Element Protocol
MDL*
Tolerance
Nicotine Concentration GC/FID Analysis
0.1 mg/ml
± 10%
Diethylene glycol (DEG) GC/FID Analysis
2.23 µg/ml (ppm)
No Detection
Acetaldehyde HPLC/UV Analysis
0.640 µg/ml (ppm)
< 100 µg/ml (ppm)
Acetoin HPLC/UV Analysis
0.841 µg/ml (ppm)
None Set (Informational)
Diacetyl
(2,3-Butanedione)
HPLC/UV Analysis
0.742 µg/ml (ppm)
Non-Detection Goal
< 22 µg/ml no disclosure
< 100 µg/ml (ppm) disclosure
> 100 µg/ml (ppm) is Fail
Formaldehyde HPLC/UV Analysis
0.846 µg/ml (ppm)
< 30 µg/mL (ppm)
Acetyl Propionyl
(2,3-
Pentanedione)
HPLC/UV Analysis
0.840 µg/ml (ppm)
Non-Detection Goal
< 45 µg/ml no disclosure
< 100 µg/ml (ppm) disclosure
> 100 µg/ml (ppm) is Fail
pH Level Karl Fischer Analysis Target Levels (Informational)
5.0 to 8.5
% Water Karl Fischer Analysis None Set (Informational)

* MDL - Minimum Detection Limit. The MDL will remain relatively constant but can vary slightly from test to test depending on the calibration of the equipment.

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05 May 2014 (0514-129)

Flavour Earl Grey Tea
2.4%
Almond Amaretto
2.4%
Watermelon
2.4%
Sample ID ECTA002-017 ECTA002-018 ECTA002-019
Enthalpy Code 0514-129-01 0514-129-02 0514-129-03
Nicotine Concentration
MDL: 0.100 mg/ml
23.8 mg/ml 23.5 mg/ml 23.7 mg/ml
Diethylene glycol (DEG)
MDL: 2.23 µg/ml
ND ND ND
Acetaldehyde
MDL: 0.640 µg/ml
2.27 µg/ml ND ND
Acetoin
MDL: 0.841 µg/ml
1.87 J µg/ml 324 µg/ml ND
Diacetyl
MDL: 0.742 µg/ml
ND 9.25 µg/ml ND
Formaldehyde
MDL: 0.549 µg/ml
6.09 µg/ml 2.99 µg/ml 1.44 J µg/ml
Pentanedione
MDL: 0.840 µg/ml
ND ND ND
pH 9.34 9.32 9.40
% Water 0.36% 0.27% 0.63%
Flavour Black Cherry
1.8%
F.V. Cappuccino
1.8%
Creamy Cappuccino
1.8%
Sample ID ECTA002-020 ECTA002-021 ECTA002-022
Enthalpy Code 0514-129-04 0514-129-05 0514-129-06
Nicotine Concentration
MDL: 0.100 mg/ml
17.7 mg/ml 17.5 mg/ml 17.3 mg/ml
Diethylene glycol (DEG)
MDL: 2.23 µg/ml
ND ND ND
Acetaldehyde
MDL: 0.640 µg/ml
ND 25.0 µg/ml 1.11 J µg/ml
Acetoin
MDL: 0.841 µg/ml
1.24 J µg/ml 8.66 µg/ml 16.2 µg/ml
Diacetyl
MDL: 0.742 µg/ml
ND ND 2.09 J µg/ml
Formaldehyde
MDL: 0.549 µg/ml
1.70 J µg/ml 1.14 J µg/ml 0.885 J µg/ml
Pentanedione
MDL: 0.840 µg/ml
ND ND ND
pH 9.15 8.56 8.73
% Water 1.20% 2.48% 3.26%
Flavour Canadian Maple
1.2%
Canadian Menthol
1.2%
Pomegranate
1.2%
Sample ID ECTA002-023 ECTA002-024 ECTA002-025
Enthalpy Code 0514-129-07 0514-129-08 0514-129-09
Nicotine Concentration
MDL: 0.100 mg/ml
11.5 mg/ml 11.4 mg/ml 18.3 mg/ml
See Actions
Diethylene glycol (DEG)
MDL: 2.23 µg/ml
ND ND ND
Acetaldehyde
MDL: 0.640 µg/ml
2.48 J µg/ml ND 1.17 J µg/ml
Acetoin
MDL: 0.841 µg/ml
3.53 J µg/ml 3.22 J µg/ml ND
Diacetyl
MDL: 0.742 µg/ml
ND ND ND
Formaldehyde
MDL: 0.549 µg/ml
1.01 J µg/ml 1.45 J µg/ml 1.40 J µg/ml
Pentanedione
MDL: 0.840 µg/ml
21.8 µg/ml ND ND
pH 8.65 9.12 8.95
% Water 0.23% 0.21% 0.21%
Flavour Chai Tea
0.8%
Banana Cream
0.8%
Blackberry Tobacco
0.8%
Sample ID ECTA002-026 ECTA002-027 ECTA002-028
Enthalpy Code 0514-129-10 0514-129-11 0514-129-12
Nicotine Concentration
MDL: 0.100 mg/ml
7.41 mg/ml 7.84 mg/ml 7.23 mg/ml
Diethylene glycol (DEG)
MDL: 2.23 µg/ml
ND ND ND
Acetaldehyde
MDL: 0.640 µg/ml
11.7 µg/ml ND ND
Acetoin
MDL: 0.841 µg/ml
3.29 J µg/ml 821 µg/ml 2.17 J µg/ml
Diacetyl
MDL: 0.742 µg/ml
ND 16.7 µg/ml ND
Formaldehyde
MDL: 0.549 µg/ml
2.34 µg/ml 3.87 µg/ml 1.49 J µg/ml
Pentanedione
MDL: 0.840 µg/ml
ND ND ND
pH 8.66 7.83 7.14
% Water 0.53% 0.34% 0.34%
Flavour Sweet Honey Cigar
Non-Nic
French Vanilla
Non-Nic
Coconut Rum Balls
Non-Nic
Sample ID ECTA002-029 ECTA002-030 ECTA002-031
Enthalpy Code 0514-129-13 0514-129-14 0514-129-15
Nicotine Concentration
MDL: 0.100 mg/ml
ND ND ND
Diethylene glycol (DEG)
MDL: 2.23 µg/ml
ND ND ND
Acetaldehyde
MDL: 0.640 µg/ml
7.01 µg/ml NQ NQ
Acetoin
MDL: 0.841 µg/ml
1.89 J µg/ml ND 101
Diacetyl
MDL: 0.742 µg/ml
ND ND ND
Formaldehyde
MDL: 0.549 µg/ml
2.52 µg/ml 3.79 J µg/ml 1.22 J µg/ml
Pentanedione
MDL: 0.840 µg/ml
ND ND 14.8 J µg/ml
pH 5.85 5.59 5.40
% Water 0.25% 0.41% 2.66%

ND: Non Detect or analytical result below the MDL.
J: Results flagged "J" are below the Lower Curve Limit, above the MDL, and are considered estimates.
NQ: Not Quantified due to uncharacteristic peak.

ACTIONS TAKEN:

  • Pomegranate 1.2%, more than ± 10% variation - This was an issue of an incorrectly labelled test sample. The intended sample was to be a 1.2% but in double-checking the batch number for the sample sent, it was a 1.8% sample.

The pages of the report showing these results are below:

Cover Page Report Page 4 Report Page 5
Report Page 6 Report Page 7 Report Page 8
Report Page 9 Report Page 10 Report Page 11

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