E-Liquid Test Results for 25 March 2015 (0315-555) - Enthalpy Labs

E-Liquid Test Results for 25 March 2015 (0315-555) - Enthalpy Labs

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Standards Legend
Component / Element Protocol
MDL*
Tolerance
Nicotine Concentration GC/FID Analysis
0.1 mg/ml
± 10%
Diethylene glycol (DEG) GC/FID Analysis
2.23 µg/ml (ppm)
No Detection
Acetaldehyde HPLC/UV Analysis
0.640 µg/ml (ppm)
< 100 µg/ml (ppm)
Acetoin HPLC/UV Analysis
0.841 µg/ml (ppm)
None Set (Informational)
Diacetyl
(2,3-Butanedione)
HPLC/UV Analysis
0.742 µg/ml (ppm)
Non-Detection Goal
< 22 µg/ml no disclosure
< 100 µg/ml (ppm) disclosure
> 100 µg/ml (ppm) is Fail
Formaldehyde HPLC/UV Analysis
0.846 µg/ml (ppm)
< 30 µg/mL (ppm)
Acetyl Propionyl
(2,3-
Pentanedione)
HPLC/UV Analysis
0.840 µg/ml (ppm)
Non-Detection Goal
< 45 µg/ml no disclosure
< 100 µg/ml (ppm) disclosure
> 100 µg/ml (ppm) is Fail
pH Level Karl Fischer Analysis Target Levels (Informational)
5.0 to 8.5
% Water Karl Fischer Analysis None Set (Informational)

* MDL - Minimum Detection Limit. The MDL will remain relatively constant but can vary slightly from test to test depending on the calibration of the equipment.

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25 March 2015 (0315-555)

This test result contains 31 new flavours. However, we are only releasing 20 of them at this time. The ones that we are currently releasing are listed below.

Flavour Sour Rainbow
Non-Nic
Mr. Cottontail
Non-Nic
Nerd Sauce
Non-Nic
Sample ID ECTA002-078 ECTA002-079 ECTA002-080
Enthalpy Code 0315-555-01 0315-555-02 0315-555-03
Nicotine Concentration
MDL: 0.100 mg/ml
ND ND ND
Diethylene glycol (DEG)
MDL: 4.45 µg/ml
ND ND ND
Acetaldehyde
MDL: 0.640 µg/ml
9.89 µg/ml 44.0 µg/ml 30.7 µg/ml
Acetoin
MDL: 0.841 µg/ml
ND 147 µg/ml ND
Diacetyl
MDL: 0.742 µg/ml
9.74 µg/ml 3.55 J µg/ml 16.7 µg/ml
Formaldehyde
MDL: 0.549 µg/ml
3.07 µg/ml 3.15 J µg/ml 2.78 J µg/ml
Pentanedione
MDL: 0.840 µg/ml
ND ND ND
pH 3.89 4.55 4.13
% Water 1.12% 1.56% 0.79%
Flavour Cocoa Razz
Non-Nic
O.C. Fizzin'
Non-Nic
Melon Dramatic
Non-Nic
Sample ID ECTA002-081 ECTA002-083 ECTA002-085
Enthalpy Code 0315-555-04 0315-555-06 0315-555-08
Nicotine Concentration
MDL: 0.100 mg/ml
ND MD ND
Diethylene glycol (DEG)
MDL: 2.23 µg/ml
ND ND ND
Acetaldehyde
MDL: 0.640 µg/ml
43.0 µg/ml 21.2 µg/ml 17.3 µg/ml
Acetoin
MDL: 0.841 µg/ml
42.8 µg/ml 2.40 J µg/ml 2.60 J µg/ml
Diacetyl
MDL: 0.742 µg/ml
2.03 J µg/ml 2.49 J µg/ml 57.0 J µg/ml
See Actions
Formaldehyde
MDL: 0.549 µg/ml
3.35 µg/ml 4.38 µg/ml 1.73 J µg/ml
Pentanedione
MDL: 0.840 µg/ml
ND ND ND
pH 3.95 3.75 4.56
% Water 1.35% 2.20% 0.59%
Flavour Diner Floats
Non-Nic
County Fair
Non-Nic
Tickin' Out
Non-Nic
Sample ID ECTA002-087 ECTA002-088 ECTA002-089
Enthalpy Code 0315-555-10 0315-555-11 0315-555-12
Nicotine Concentration
MDL: 0.100 mg/ml
ND ND ND
Diethylene glycol (DEG)
MDL: 2.23 µg/ml
ND ND ND
Acetaldehyde
MDL: 0.640 µg/ml
34.1 µg/ml 21.1 µg/ml 21.6 µg/ml
Acetoin
MDL: 0.841 µg/ml
ND 47.5 µg/ml ND
Diacetyl
MDL: 0.742 µg/ml
ND ND ND
Formaldehyde
MDL: 0.549 µg/ml
3.62 J µg/ml 3.59 µg/ml 4.66 µg/ml
Pentanedione
MDL: 0.840 µg/ml
ND 20.4 µg/ml ND
pH 5.86 5.67 5.98
% Water 0.95% 3.21% 1.77%
Flavour Heaven's Gate
Non-Nic
#RedGreen
Non-Nic
Berry Royale
Non-Nic
Sample ID ECTA002-093 ECTA002-094 ECTA002-095
Enthalpy Code 0315-555-16 0315-555-17 0315-555-18
Nicotine Concentration
MDL: 0.100 mg/ml
ND ND ND
Diethylene glycol (DEG)
MDL: 2.23 µg/ml
ND ND ND
Acetaldehyde
MDL: 0.640 µg/ml
17.0 µg/ml 15.2 µg/ml 5.11 µg/ml
Acetoin
MDL: 0.841 µg/ml
ND ND 7.80 µg/ml
Diacetyl
MDL: 0.742 µg/ml
ND 1.96 J µg/ml 1.70 J µg/ml
Formaldehyde
MDL: 0.549 µg/ml
3.46 µg/ml 4.55 µg/ml 4.19 µg/ml
Pentanedione
MDL: 0.840 µg/ml
ND ND ND
pH 5.02 4.51 4.70
% Water 0.70% 1.54% 3.06%
Flavour Grandma's House
Non-Nic
Froopz
Non-Nic
Date Night
Non-Nic
Sample ID ECTA002-096 ECTA002-097 ECTA002-098
Enthalpy Code 0315-555-19 0315-555-20 0315-555-21
Nicotine Concentration
MDL: 0.100 mg/ml
ND ND ND
Diethylene glycol (DEG)
MDL: 2.23 µg/ml
ND ND ND
Acetaldehyde
MDL: 0.640 µg/ml
9.42 µg/ml 27.6 µg/ml 21.2 µg/ml
Acetoin
MDL: 0.841 µg/ml
170 µg/ml 105 µg/ml ND
Diacetyl
MDL: 0.742 µg/ml
2.34 J µg/ml 2.10 J µg/ml ND
Formaldehyde
MDL: 0.549 µg/ml
3.56 µg/ml 6.61 µg/ml 5.32 µg/ml
Pentanedione
MDL: 0.840 µg/ml
2.94 J µg/ml 18.2 J µg/ml ND
pH 5.18 5.51 4.76
% Water 2.36% 1.46% 1.01%
Flavour Feck Off
Non-Nic
Tiger Tailz
Non-Nic
Sapphire Slush
Non-Nic
Sample ID ECTA002-099 ECTA002-100 ECTA002-101
Enthalpy Code 0315-555-22 0315-555-23 0315-555-24
Nicotine Concentration
MDL: 0.100 mg/ml
ND ND ND
Diethylene glycol (DEG)
MDL: 2.23 µg/ml
ND ND ND
Acetaldehyde
MDL: 0.640 µg/ml
13.3 µg/ml 32.9 µg/ml 16.7 J µg/ml
Acetoin
MDL: 0.841 µg/ml
410 µg/ml 61.7 µg/ml 74.6 µg/ml
Diacetyl
MDL: 0.742 µg/ml
6.21 µg/ml ND ND
Formaldehyde
MDL: 0.549 µg/ml
6.07 µg/ml 8.80 µg/ml 3.11 µg/ml
Pentanedione
MDL: 0.840 µg/ml
ND 9.44 µg/ml 13.3 µg/ml
pH 5.12 5.18 5.24
% Water 1.82% 1.56% 1.57%
Flavour Secret Affair
Non-Nic
Supernova
Non-Nic
Fat Elvis
Non-Nic
Sample ID ECTA002-102 ECTA002-104 ECTA002-105
Enthalpy Code 0315-555-25 0315-555-27 0315-555-28
Nicotine Concentration
MDL: 0.100 mg/ml
ND ND 0.0980 mg/ml
See Actions
Diethylene glycol (DEG)
MDL: 2.23 µg/ml
ND ND ND
Acetaldehyde
MDL: 0.640 µg/ml
4.20 J µg/ml 5.34 µg/ml 45.4 µg/ml
Acetoin
MDL: 0.841 µg/ml
ND 10.6 µg/ml 86.2 µg/ml
Diacetyl
MDL: 0.742 µg/ml
ND 4.71 µg/ml 3.92 µg/ml
Formaldehyde
MDL: 0.549 µg/ml
3.29 µg/ml 5.68 µg/ml 5.52 µg/ml
Pentanedione
MDL: 0.840 µg/ml
4.93 µg/ml 15.4 µg/ml ND
pH 5.66 5.08 5.28
% Water 1.02% 2.57% 0.55%

ND: Non Detect or analytical result below the MDL.
J: Results flagged "J" are below the Lower Curve Limit, above the MDL, and are considered estimates.
NQ: Not Quantified due to uncharacteristic peak.

ACTIONS TAKEN:

  • Melon Dramatic, Diacetyl Detection more than 22 ppm - We believe this to be a cross-contamination and are retesting immediately.
  • Fat Elvis, exceeds ± 10% threshold - We suspect a cross contamination with one of the flavourings and are reviewing our processes to ensure that this is corrected.

The pages of the report showing these results are below. The report itself contains 31 new flavours but only 20 of them are currently being released. Those flavours that are released have been highlighted in yellow:

Flavour Translation Cover Page Report Page 4
Report Page 5 Report Page 6 Report Page 7
Report Page 8 Report Page 15 Report Page 16
Report Page 17

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